Review Team (February 2016)

Fonterra Co-operative Group VitD-18 (February 2016) FOR ERP USE ONLY DO NOT DISTRIBUTE

Table D9: Data vitamin D 3

100% recovery experiment 2

(μg hg -1 )

Vitamin D 2

Recovery (%)

Sample

Units

Unspiked sample

Spiked sample

Spike

μg hg -1 μg hg -1

Child Formula Powder Infant Elemental Powder

0.0 0.0 0.0 0.0 0.0

10.2

10.0 10.0 20.0 20.0 20.0

101.8

9.9

98.8 98.3 99.9 98.5

μg L -1 μg L -1 μg L -1

Adult Nutritional RTF High Protein Adult Nutritional RTF High Fat Infant Formula RTF, Milk-Based

19.7 20.0 19.7

Table D10: Data vitamin D 3

50% recovery experiment 2

(μg hg -1 )

Vitamin D 2

Recovery (%)

Sample

Units

Unspiked sample

Spiked sample

Spike

μg hg -1 μg hg -1

Child Formula Powder Infant Elemental Powder

0.0 0.0 0.0 0.0 0.0

5.0 4.8 9.6

4.9 4.9 9.8 9.8 9.8

101.5

96.9 98.0

μg L -1 μg L -1 μg L -1

Adult Nutritional RTF High Protein Adult Nutritional RTF High Fat Infant Formula RTF, Milk-Based

10.2

104.1

9.2

93.9

Table D11: Data vitamin D 3

100% recovery experiment 3

(μg hg -1 )

Vitamin D 2

Recovery (%)

Sample

Units

Unspiked sample

Spiked sample

Spike

μg hg -1 μg hg -1

Child Formula Powder Infant Elemental Powder

0.0 0.0 0.0 0.0 0.0

10.1

9.9 9.9

101.5

9.8

98.7 98.2

μg L -1 μg L -1 μg L -1

Adult Nutritional RTF High Protein Adult Nutritional RTF High Fat Infant Formula RTF, Milk-Based

19.5 19.9 19.3

19.9 19.9 19.9

100.1

97.4

Table D12: Data vitamin D 3

50% recovery experiment 3

(μg hg -1 )

Vitamin D 2

Recovery (%)

Sample

Units

Unspiked sample

Spiked sample

Spike

μg hg -1 μg hg -1

Child Formula Powder Infant Elemental Powder

0.0 0.0 0.0 0.0 0.0

5.0 4.7 9.6

4.9 4.9 9.7 9.7 9.7

101.5

95.4 98.7

μg L -1 μg L -1 μg L -1

Adult Nutritional RTF High Protein Adult Nutritional RTF High Fat Infant Formula RTF, Milk-Based

10.1

103.3

9.1

93.8

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