Review Team (February 2016)

VitD-18 (February 2016) FOR ERP USE ONLY DO NOT DISTRIBUTE

Table 3: Precision—Repeatability and intermediate precision

Replicates (n)

SMPR Requirements

RSD r

RSD iR

RSD r

RSD iR

Product

SPIFAN Code

Analyte

Conc. Level

Concentration

1.2 μg hg -1 RTF 1.1 μg hg -1 RTF 1 μg hg -1 RTF 0.9 μg hg -1 RTF 0.9 μg hg -1 RTF 1.2 μg hg -1 RTF 1.1 μg hg -1 RTF 1 μg hg -1 RTF 0.9 μg hg -1 RTF 0.9 μg hg -1 RTF 0.9 μg hg -1 RTF 0.4 μg hg -1 RTF 0.9 μg hg -1 RTF 0.9 μg hg -1 RTF 0.8 μg hg -1 RTF 1.1 μg hg -1 RTF 1.1 μg hg -1 RTF 0.7 μg hg -1 RTF 1 μg hg -1 RTF 1.3 μg hg -1 RTF Global Mean %

0.12 μg hg -1 RTF 1.5 μg hg -1 RTF 2.5 μg hg -1 RTF 5.1 μg hg -1 RTF

Child Formula Powder Infant Elemental Powder

00847RF00

3 3 3 3 3

– – – – –

≤15

5.4% 5.4% 7.4% 5.0% 4.4% 5.4% 5.4% 7.4% 5.0% 4.4% 4.4% 6.3% 5.8% 3.1% 4.7% 6.4% 3.6% 7.8% 5.2% 7.9% 5.0%

00796RF

Vitamin D

No limit set

(1)

≤11

Vitamin D 2

Adult Nutritional RTF High Protein Adult Nutritional RTF High Fat Infant Formula RTF, Milk-Based In-House Reference IF Powder IF Powder Part. Hydrolysed Milk-Based IF Powder Part. Hydrolysed Soy-Based Toddler Formula Powder Milk-Based Infant Formula Powder Milk-Based Adult Nutritional Powder Low Fat NIST SRM1849a Infant Formula Powder FOS/GOS-Based Infant Formula Powder Milk-Based Infant Formula Powder Soy-Based Infant Formula RTF Milk-Based Adult Nutritional RTF High Protein Adult Nutritional RTF High Fat Child Formula Powder Infant Elemental Powder

00821RF00 00820RF00

EV4H2Q

5.2% 2.8% 4.4% 1.8% 2.2% 2.1% 3.7% 3.3% 3.5% 1.5% 3.3% 2.6% 2.3% 1.6% 4.9% 3.0%

—

12 12 12 12 12 12 12 12 12 12 12 12 12 12 12

CLC10-b

410057652Z 410457651Z 4052755861 4044755861 00859RF00 00866RF00

Vitamin D 3

00795RF

50350017W1

K16NTAV E10NWZC

EV4H2R

00730RF00 00729RF00

Footnotes:

(1) Estimated from spiked recovery study, intermediate precision only, no repeability data available

SPIFAN ERP X Checklist v 1.0