SPDS SET 2: ASH-01
NATURAL REMEDIES PVT LIMITED QUALITY CONTROL DEPARTMENT
Acquired by Sample Name
: Admin
: Withania somnifera : WS / 06 lot 10
Sample ID
: 2500 mg / 100 ml : Trl 2
Vail #
: 39
Injection Volume Data File Name Method File Name Batch File Name Report File Name Data Acquired Data Processed
: 20 uL
: Rep-RP010.lcd : Withaina.met.lcm : Batch 01.lcb : Calibration.lcr
: 1/16/2007 8:25:06 AM : 1/23/2007 3:18:58 AM
D:\LC2010AHT\2007\Method validation\Withania somnifera\Jan 2007\Rep-RP010.lcd
mV
1Det.A Ch1
3
500
1
4
250
5
2
6
0
0
5
10
15
20
25
30
35
40
45
min
Det.A Ch1/227nm 1
Detector A Ch1 227nm Peak # Ret. Time
Area 1546771 1271665 3508268 1767374 1279368 393606 9767052
Height
Area %
Name
1 2 3 4 5 6 Total
15.463 19.621 20.302 21.325 22.189 25.490
272883 183718 491917 288311 225079 70117 1532025
15.837 13.020 35.919 18.095 13.099 4.030 100.000
Withanoside IV Withanoside V Withaferin A 12- Deoxy withastramonolide
Withanollide A Withanolide B
D:\LC2010AHT\2007\Method validation\Withania somnifera\Jan 2007\Rep-RP010.lcd
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