SPDS SET 2: ASH-01

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Sample ID : Withania somnifera : WS - 06 lot 10 Method Name

: C:\CLASS-VP\Methods\METHODS\Withania.met

Data Name

: D:\2007\Method validation\Withania somnifera\Jan 2007\160107\spl-16

Injection Volume

: 20

Acquired

: 1/17/07 6:41:54 AM

500

500

400

400

21.440

300

300

mAU

mAU

16.576

200

200

22.400

23.243

20.672

100

100

26.496

0

0

0

5

10

15

20

25

30

35

40

45

Minutes

Detector A-227 nm Retention Time

Area Area

Resolution Asymmetry Theoretica l plates

Capacity factor

Width USP Width

Height

Percent

16.576 20.672

998797 17.55 745691 13.11

0.00

1.04 1.02 1.13 1.04 1.02 1.19

137409.30 -0.04 177685.13 0.20 182807.92 0.24 243337.77 0.30 296866.34 0.35 406992.84 0.54

0.24 0.18 159064 0.30 0.20 104250 0.34 0.20 275305 0.25 0.18 146645 0.22 0.17 127311 0.22 0.17 37559

21.84

21.440 2024836 35.59

3.87 5.02 4.78

22.400 23.243 26.496

940711 16.53 757964 13.32 221905 3.90

19.32

Totals

5689904 100.00

850134

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