SPIFAN Nutrients ERP Book_9-29-15

GOS-02 SLV FOR ERP USE ONLY DO NOT DISTRIBUTE

Single Lab Validation Report for GOS in Infant Formula and Adult Nutritionals

Table of Contents 1 Introduction .................................................................................................................................... 3

2 Methodology and trials.................................................................................................................... 4

2.1 Samples ................................................................................................................................... 4

2.2 Method.................................................................................................................................... 5

2.3 Validation Design ..................................................................................................................... 5

2.3.1

Linearity ........................................................................................................................... 5

2.3.2

Precision........................................................................................................................... 5

2.3.3

Accuracy........................................................................................................................... 5

3 Results............................................................................................................................................. 6

3.1 Linearity................................................................................................................................... 6

3.2 Precision ................................................................................................................................ 10

3.3 Accuracy ................................................................................................................................ 10

4 Conclusions ................................................................................................................................... 12

5 Appendices.................................................................................................................................... 13

5.1 Detailed Method Description ................................................................................................. 13

5.2 Raw data – Method Precision................................................................................................. 21

5.3 Raw data – Method accuracy ................................................................................................. 21

5.4 Example chromatograms........................................................................................................ 26

2