SPIFAN Nutrients ERP Book_9-29-15

Carn-06 - Validation Report FOR ERP USE ONLY DO NOT DISTRIBUTE

Appendix 2: Precision

Anava: Single Factor

Carnitine (mg/kg) Matrix: Milk powder

SUMMARY

Replicate 1 Replicate 2

Groups

Count

Sum

Average

Variance

day 1 day 2 day 3 day 4 day 5 day 6 day 7 day 8 day 9

96,110 99,537 97,998 98,114 98,540 100,585 95,046 98,207 90,559 95,917 99,272 93,529 92,832 91,049 92,619 92,152

95,648 95,202 97,719 93,736 98,514 93,959 95,060 94,833 96,481 89,388 99,268 93,463 92,560 91,474 95,317 95,635

day 1 day 2 day 3 day 4 day 5 day 6 day 7 day 8 day 9 day 10 day 11 day 12 day 13 day 14 day 15 day 16

2 191,758

95,879

0,106722

2 194,739 97,3695 9,3961125 2 195,717 97,8585 0,0389205

2 191,85 2 197,054 2 194,544 2 190,106 2 193,04 2 187,04 2 198,54 2 186,992 2 185,392

95,925 98,527

9,583442 0,000338

97,272 21,951938

95,053

9,8E-05 5,691938

96,52

93,52 17,535042

day 10 day 11 day 12 day 13 day 14 day 15 day 16

2 185,305 92,6525 21,3139205

99,27

8E-06

93,496 92,696

0,002178 0,036992

2 182,523 91,2615 0,0903125

2 187,936

93,968

3,639602

2 187,787 93,8935 6,0656445

Average of all days

95,32 mg/kg

ANAVA Source of Variation Between Groups

SS

df

MS

F

P-value

F crit

166,8678192 15 11,12452128 1,86470778 0,113837078 2,352222763

Within Groups

95,4532085 16 5,965825531

Total

262,3210277 31

Anava: Single Factor

Carnitine (mg/kg) Matrix: pet food

SUMMARY

Replicate 1 Replicate 2

Groups

Count

Sum

Average

Variance

day 1 day 2 day 3 day 4 day 5 day 6 day 7 day 8 day 9

357,418 346,842 342,908 348,298 353,781 318,183 365,650 363,560 366,707 336,970 342,770 348,137 343,212 330,134

352,315 347,401 354,980 351,989 360,330 336,589 368,775 361,314 349,201 341,202 349,700 335,804 344,259 343,909

day 1 day 2 day 3 day 4 day 5 day 6 day 7 day 8 day 9 day 10 day 11 day 12 day 13 day 14

2 709,733 354,8665 13,0203045 2 694,243 347,1215 0,1562405 2 697,888 348,944 72,866592 2 700,287 350,1435 6,8117405 2 714,111 357,0555 21,4447005 2 654,772 327,386 169,390418 2 734,425 367,2125 4,8828125

2 724,874 362,437

2,522258

2 715,908 357,954 153,230018

day 10 day 11 day 12 day 13 day 14

2 678,172 339,086 2 692,47 346,235

8,954912 24,01245

2 683,941 341,9705 76,0514445 2 687,471 343,7355 0,5481045 2 674,043 337,0215 94,8753125