SPIFAN Nutrients ERP Book_9-29-15

Carn-06 (Validation Report-Addendum) FOR ERP USE ONLY DO NOT DISTRIBUTE

Rep. 1 (mg/kg) Rep. 2 (mg/kg) 134,697865 128,2971403 129,6820154 135,5318291 126,3429604 130,0314128

Average of all days 130,76 mg/kg

Day 1 Day 2 Day 3

Anava: Single faktor Summary Groups

Count

Sum

Average

Variance

Day 1 Day 2 Day 3

2 262,9950053 131,4975027 20,48464 2 265,2138445 132,6069223 17,11016 2 256,3743732 128,1871866 6,80234

ANAVA Source of Variation

SS

df

MS

F

P-value

F crit

Between Groups Within Groups

21,14871193 44,39713863 65,54585056 -2,112345122 12,68670109

2 10,57435596 3 14,79904621

0,71453 0,557461227 9,552094496

Total Sl^2 SR^2

5

Reproducibility (SR) Repeatability (Sr)

3,561839565 mg/kg 3,846952847 mg/kg

RSD%

2,7 % 2,9 %

Sample name: Adult Nut. Protein Based Eurofins Sample nr.: 487-2014-04020192

Rep. 1 (mg/kg) Rep. 2 (mg/kg) 0,559860736 0,546500224 0,634757888 0,556387636 0,63121476 0,433868339

Average of all days

Day 1 Day 2 Day 3

0,56 mg/kg

Anava: Single faktor Summary Groups

Count

Sum

Average

Variance

Day 1 Day 2 Day 3

2

1,10636096

0,55318048 8,93E-05

2 1,191145524 0,595572762 0,003071 2 1,065083099 0,532541549 0,019473

ANAVA Source of Variation

SS

df

MS

F

P-value

F crit

Between Groups Within Groups

0,00413067 0,022633005 0,026763674 -0,0027395 0,004804835

2 0,002065335 3 0,007544335

0,27376 0,777668862 9,552094496

Total Sl^2 SR^2

5

Reproducibility (SR) Repeatability (Sr)

0,069316916 mg/kg 0,086858131 mg/kg

RSD%

12,4 % 15,5 %

Sample name: Infant Formula, Part. Hyd. Milk

Eurofins Sample nr.: 487-2014-04020193

Rep. 1 (mg/kg) Rep. 2 (mg/kg) 82,51960816 82,99928787

Average of all days 81,91 mg/kg

Day 1 Day 2 Day 3

82,19875801

80,2750676

85,21276187 78,25727551