SPIFAN Nutrients ERP Book_9-29-15

GOS-02 SLV FOR ERP USE ONLY DO NOT DISTRIBUTE

Single Lab Validation Report for GOS in Infant Formula and Adult Nutritionals

Spike-Recovery: Sample 12 Infant Elemental Powder

GOS Spike Level Measured GOS Recovery Average RSD (g/100g) (g/100g) (%) (%) (%)

Date* Instrument** GOS

11-02-2015 ICS 3000 11-02-2015 ICS 3000 19-02-2015 ICS 5000 19-02-2015 ICS 5000 10-06-2015 ICS 3000 10-06-2015 ICS 3000 11-02-2015 ICS 3000 11-02-2015 ICS 3000 19-02-2015 ICS 5000 19-02-2015 ICS 5000 10-06-2015 ICS 3000 10-06-2015 ICS 3000 11-02-2015 ICS 3000 11-02-2015 ICS 3000 19-02-2015 ICS 5000 19-02-2015 ICS 5000 10-06-2015 ICS 3000 10-06-2015 ICS 3000 11-02-2015 ICS 3000 11-02-2015 ICS 3000 19-02-2015 ICS 5000 19-02-2015 ICS 5000 10-06-2015 ICS 3000 10-06-2015 ICS 3000

0.022 0.022 0.023 0.023 0.023 0.023 0.124 0.124 0.124 0.124 0.127 0.127 0.397 0.397 0.415 0.415 0.401 0.401 0.564 0.564 0.561 0.561 0.561 0.561

0.015 0.019 0.016 0.016 0.014 0.016 0.107 0.110 0.094 0.095 0.085 0.090 0.329 0.339 0.352 0.348 0.352 0.372 0.501 0.512 0.484 0.514 0.408 0.430

67 84 71 70 63 71 86 88 76 76 67 71 83 86 85 84 88 93 89 91 86 91 73 77

Clasado

71

10.3

Vivinal

78

10.7

Clasado

86

4.1

Vivinal

84

9.3

* Date = date of preparative separation ** Instrument = instrument used for quantification

25