SPIFAN Nutrients ERP Book_9-29-15

Carn-06 (Validation Report-Addendum) FOR ERP USE ONLY DO NOT DISTRIBUTE

Total Sl^2 SR^2

0,398811116 0,017261779 0,083214579

5

Reproducibility (SR) Repeatability (Sr)

0,29 mg/kg 0,26 mg/kg

RSD%

30,2 % 26,9 %

Sample name Infant Formula, Part. Hyd. Milk Sample nr. 487-2014-04020193

Rep 1 (mg/kg) Rep 2 (mg/kg) 101,7408897 102,7245457 105,950458 109,4827952 108,560353 103,1222465

Average of all days

Day 1 Day 2 Day 3

105,26 mg/kg

Anava: Single faktor Summary Groups

Count

Sum

Average

Variance

Day 1 Day 2 Day 3

2 204,4654354 102,2327177 0,483789567 2 215,4332532 107,7166266 6,238703172

2 211,6825994 105,8412997

14,786501

ANAVA Source of Variation

SS

df

MS

F

P-value

F crit

Between Groups Within Groups

31,07464766 21,50899374 52,5836414 4,183829625 11,3534942

2 15,53732383 2,16709215 0,26161 9,552094

3 7,16966458

Total Sl^2 SR^2

5

Reproducibility (SR) Repeatability (Sr)

3,37 mg/kg 2,68 mg/kg

RSD%

3,2 % 2,5 %

Sample name Infant Formula, Part. Hyd. Soy Sample nr. 487-2014-04020194

Rep 1 (mg/kg) Rep 2 (mg/kg) 92,0471692 92,14563536 94,53785472 91,33048028 94,638898 94,85876736

Average of all days

Day 1 Day 2 Day 3

93,26 mg/kg

Anava: Single faktor Summary Groups

Count

Sum

Average

Variance

Day 1 Day 2 Day 3

2 184,1928046 92,09640228 0,004847792 185,868335 92,9341675 5,143625387 2 189,4976654 94,74883268 0,024171269 2

ANAVA Source of Variation

SS

df

MS

F

P-value

F crit

Between Groups Within Groups

7,353498227 5,172644447 12,52614267 0,976267149 2,700481965

2 3,676749113 2,132419394 0,265365 9,552094

3 1,724214816

Total Sl^2 SR^2

5

Reproducibility (SR)

1,64 mg/kg

RSD%

1,8 %