SPSFAM Meeting eBook March 2017

93 94

Table 2: Method performance requirements (part 1).

Requirement THC, THCA, CBDA, CBD, Individually Reported

Requirement (Additional, Desirable Cannabinoids (Table 1b), including CBN)

Parameter

Limit of Quantitation (LOQ) (% w/w)

≤ 0.3

≤ 0.3

Analytical Range (% w/w)

≤ 0.3 – ca. 100

≤ 0.3 – ca. 50

95 96 97 98 99

*Reported as individual cannabinoids

100 101 102 103 104 105 106

Table 3: Method performance requirements (part 2).

Ranges (% w/w)

Parameters

≤ 0.3 – 1

> 1 - 10

> 10 – ca. 100

Recovery (% w/w)

95 – 105

97 - 103

98 - 102

% RSD r

≤ 5 ≤ 7

≤ 4 ≤ 5

≤ 2 ≤ 3

% RSD R