SPSFAM ERP

Table AI-2-3 . Lemon Juice Sucrose Spike Results

Spike Level Added (%)

Approx. Spiking level (%)

Average Innate level (%)

Mean Recovery n=3 (%)

Mean Recovery (%)

Measured Result (%)

Total Recovery (%)

%RSD r n=3

%RSD R n=12

Site

Sample ID

BC BC BC

6196413 6196414 6196415 6345733 6345734 6345735

0.496 0.496 0.495 0.494 0.497 0.494 0.505 0.505 0.497 0.495 0.491 0.503 0.776 0.782 0.779 0.786 0.795 0.792 0.799 0.800 0.802 0.800 0.792 0.802

0.475 0.476 0.486 0.496 0.499 0.491 0.501 0.506 0.500 0.478 0.483 0.480 0.760 0.778 0.765 0.798 0.778 0.797 0.799 0.800 30.33 0.781 0.776 0.771

95.8 96.0 98.2

0.000

96.7

1.4

HAR HAR HAR MSN MSN MSN SGP SGP SGP HAR HAR HAR MSN MSN MSN SGP SGP SGP BC BC BC

100.4 100.4

0.000

100.1

0.6

99.4 99.2

0.5

98.4

2.0

5907383-1 5907383-2 5907383-3 5907383-1 5907383-2 5907383-3

100.2 100.6

0.000

100.0

0.7

96.6 98.4 95.4 97.9 99.5 98.2

0.000

96.8

1.6

6196416 6196417 6196418 6345736 6345737 6345738

0.000

98.5

0.9

101.5

97.9

0.000

100.0

1.9

100.6 100.0 100.0

0.75

98.8

1.6

5907383-4 5907383-5 5907383-6 5907383-4 5907383-5 5907383-6

0.000

100.0

0.0

3783.9

97.6 98.0 96.1

0.000

97.2

1.0

Bold type indicates outlier omitted from data summary.