SPSFAM ERP

Table AI-2-4 . Lemon Juice Fructose Spike Results

Spike Level Added (%) 0.498 0.498 0.497 0.495 0.498 0.494 0.504 0.504 0.496 0.497 0.493 0.506 0.779 0.785 0.783 0.787 0.796 0.793 0.797 0.798 0.800 0.804 0.796 0.806

Approx. Spiking level (%)

Average Innate level (%)

Mean Recovery n=3 (%)

Measured Result (%)

Total Recovery (%)

%RSD r n=3

Mean Recovery

%RSD R n=12

Site

Sample ID

BC BC BC

6196413 6196414 6196415 6345733 6345734 6345735

0.876 0.888 0.887 0.875 0.864 0.855 0.905 0.912 0.907 0.884 0.870 0.878

99.0

100.3 100.3

0.387

99.9

0.8

HAR HAR HAR MSN MSN MSN SGP SGP SGP HAR HAR HAR MSN MSN MSN SGP SGP SGP BC BC BC

99.7 98.1 97.5

0.383

98.4

1.2

0.9

99.2

1.4

5907383-1 5907383-2 5907383-3 5907383-1 5907383-2 5907383-3

100.0 100.8 101.1

0.401

100.6

0.6

98.9 97.8 97.2

0.397

98.0

0.9

6196416 6196417 6196418 6345736 6345737 6345738

1.18 1.17 1.20 1.15 1.13 1.14 1.21 1.20 1.30 1.17 1.18 1.18

101.2

99.8

0.387

101.2

1.4

102.6

98.3 95.8 96.9

0.383

97.0

1.3

1.25

99.1

2.1

5907383-4 5907383-5 5907383-6 5907383-4 5907383-5 5907383-6

101.0 100.1 108.2

0.401

100.6

0.6

97.4 98.9 98.1

0.397

98.1

0.8

Bold type indicates outlier omitted from data summary