SPSFAM ERP

Table AI-2-5 . Lemon Juice Lactose Spike Results

Spike Level Added (%) 0.495 0.496 0.494 0.487 0.491 0.487 0.502 0.502 0.494 0.497 0.493 0.506 0.775 0.780 0.778 0.776 0.785 0.782 0.795 0.796 0.798 0.803 0.796 0.806

Approx. Spiking level (%)

Average Innate level (%)

Mean Recovery n=3 (%)

Measured Result (%)

Total Recovery (%)

%RSD r n=3

Mean Recovery

%RSD R n=12

Site

Sample ID

6196413 6196414 6196415 6345733 6345734 6345735

0.471 0.468 0.483 0.492 0.483 0.472 0.489 0.488 0.505 0.482 0.475 0.506 0.757 0.769 0.759 0.764 0.782 0.769 0.765 0.797 0.768 0.781 0.810 1.45

95.2 94.4 97.8 98.4 96.9 97.4 97.2 101.0 102.2

BC BC BC

0.000

95.8

1.6

HAR HAR HAR MSN MSN MSN SGP SGP SGP HAR HAR HAR MSN MSN MSN SGP SGP SGP BC BC BC

0.000

98.8

2.1

0.5

97.8

2.3

5907383-1 5907383-2 5907383-3 5907383-1 5907383-2 5907383-3

0.000

98.9

2.9

97.0 96.3

0.000

97.8

2.0

100.0

6196416 6196417 6196418 6345736 6345737 6345738

97.7 98.6 97.6 98.5 99.6 98.3 96.2

0.000

98.0

0.6

0.000

98.8

0.7

0.75

98.3

1.5

5907383-4 5907383-5 5907383-6 5907383-4 5907383-5 5907383-6

100.1 182.3

0.000

98.2

2.8

95.6 98.1

0.000

98.1

2.5

100.5

Bold type indicates outlier omitted from data summary.