SPSFAM ERP

Table AI-2-6 . Lemon Juice Isomaltulose Spike Results

Spike Level Added (%) 0.470 0.470 0.469 0.472 0.475 0.472

Approx. Spiking level (%)

Average Innate level (%)

Mean Recovery n=3 (%)

Measured Result (%)

Total Recovery (%)

%RSD r n=3

Mean Recovery

%RSD R n=12

Site

Sample ID

BC BC BC

6196413 6196414 6196415 6345733 6345734 6345735 5907383- 1 5907383- 2 5907383- 3 5907383- 1 5907383- 2 5907383- 3 6196416 6196417 6196418 6345736 6345737 6345738 5907383- 4 5907383- 5 5907383- 6 5907383- 4 5907383- 5 5907383- 6

0.476 0.479 0.489 0.506 0.497 0.486

101.3 101.9 104.3 107.2 104.6 103.0

0.000

102.5

1.6

HAR HAR HAR

0.000

104.9

2.0

MSN

0.479

0.510

106.5

0.5

103.6

2.9

0.479

0.514

107.3

MSN

0.000

106.4

0.9

MSN

0.472

0.497

105.3

SGP

0.475

0.476

100.2

SGP

0.471

0.459

97.5

0.000

100.6

3.3

SGP

0.483

0.503

104.1

BC BC BC

0.734 0.740 0.738 0.751 0.760 0.757

0.753 0.757 0.751 0.796 0.761 0.786

102.6 102.3 101.8 106.0 100.1 103.8

0.000

102.2

0.4

HAR HAR HAR

0.000

103.3

2.9

MSN

0.758

0.799

105.4

0.75

102.9

2.0

0.759

0.802

105.7

MSN

0.000

105.6

0.2

1.62

212.5

MSN

0.761

0.768

0.773

100.7

SGP

0.000

101.5

0.8

SGP

0.760

0.772

101.6

SGP

0.770

0.788

102.3

Bold type indicates outlier omitted from data summary.