SPSFAM ERP
Table AI-2-8 . Peanut butter Galactose and Glucose Spike Results Analyte Site Sample ID
Approx. Spiking level (%)
Actual Spiking level (%) 0.0967 0.0972 0.0976
Average Innate level (%)
Total Recovery (%)
Average Recovery n=3 (%)
Average Recovery n=6 (%)
%RSD r
%RSD R
Measured Result (%)
n=3
n=6
6877812 6877814 6877815 5907387‐ 1 5907387‐ 2 5907387‐ 3 6877816 6877817 6877818 5907387‐ 4 5907387‐ 5 5907387‐ 6 6877812 6877814 6877815 5907387‐ 1 5907387‐ 2 5907387‐ 3 6877816 6877817 6877818 5907387‐ 4 5907387‐ 5 5907387‐ 6
0.0899 0.0861 0.0918 0.0969
93.0 88.6 94.1 95.9
HAR
0
91.9
3.2
0.101
0.1
95.4
5.3
SGP
0.102
0.106
103.9
0
98.9
4.4
0.0990
0.0955
96.9 96.6 96.6 93.9 98.7 99.3 94.6 95.1 96.9 93.5 95.1 98.5 99.8 97.2 97.5 100.0 97.8
Galactose
1.45 1.49 1.48 1.51
1.40 1.44 1.39 1.49
HAR
0
95.7
1.6
1.5
97.5
2.3
SGP
1.43
1.43
0
99.3
0.7
1.48
1.47
0.0971 0.0975 0.0980
0.132 0.133 0.136 0.131
HAR
0.0424
95.5
1.3
0.101
0.1
95.5
1.6
0.0391
95.5
2.3
SGP
0.102
0.138
0.0986
0.131
Glucose
1.46 1.49 1.49 1.51
1.48 1.53 1.49 1.51
HAR
0.0424
98.5
1.3
1.5
98.4
1.1
1.43
1.44
98.0
SGP
0.0391
98.3
1.0
1.48
1.51
99.4
Table AI-2-9 . Peanut butter Sucrose and Fructose Spike Results
Approx. Spiking level (%)
Actual Spiking level (%)
Average Innate level (%)
Measured Result (%)
Total Recovery (%)
Average Recovery n=3 (%)
Average Recovery n=6 (%)
%RSD r
%RSD R
Analyte
Site
Sample ID
n=3
n=6
7154309 7154310 7154311
9.87 10.1 9.69 9.90 9.85 9.76 14.5 14.4 14.7 14.9 14.9 14.8
20.0 20.1 19.9 20.5 20.9 20.4 23.8 24.0 24.6 25.1 25.1 25.2
99.7 99.0
HAR
10.2
99.6
0.6
100.1 102.0 104.2 102.2
10
101.2
1.9
5907387‐1 5907387‐2 5907387‐3 7154312 7154313 7154314 5907387‐4 5907387‐5 5907387‐6 6877812 6877814 6877815 5907387‐1 5907387‐2 5907387‐3 6877816 6877817 6877818 5907387‐4
SGP
10.2
102.8
1.2
Sucrose
96.4 97.6 98.8
HAR
10.2
97.6
1.2
15
98.9
1.7
100.0 100.0 100.8 91.6 96.0 96.5 98.7 98.0 97.3 97.4 95.4 95.1 100.9
SGP
10.2
100.3
0.5
0.0970 0.0975 0.0979 0.102 0.103 0.100
0.116 0.122 0.123 0.136 0.136 0.137
HAR
0.0296
94.7
2.8
0.1
96.9
3.2
SGP
0.0358
99.2
1.5
Fructose
1.46 1.49 1.49 1.53
1.45 1.48 1.45 1.49
HAR
0.0296
96.7
1.2
1.5
97.6
2.3
SGP
0.0358
98.6
3.0
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