SPSFAM ERP
Table AI-2-15 . Ham Galactose, Glucose, Sucrose, and Fructose Spike Results Analyte SAMPLE ID
Approx. Spiking level (%)
Actual Spiking level (%) 0.0967 0.0959 0.0979 0.0970 0.0961
Average Innate level (%)
Measured Result (%)
Total Recovery (%)
Mean Recovery n=5 (%)
%RSD i n=5
6669085 6669086 6669087 6692728 6695113 6669088 6669089 6669090 6692729 6695114 6669085 6669086 6669087 6692728 6695113 6669088 6669089 6669090 6692729 6695114 6669085 6669086 6669087 6692728 6695113 6669088 6669089 6669090 6692729 6695114 6669085 6669086 6669087 6692728 6695113 6669088 6669089 6669090 6692729 6695114
0.0930 0.0923 0.0932 0.0890 0.0927
96.2 96.2 95.2 91.8 96.5
0.1
95.2
2.1
Galactose
0
1.44 1.50 1.49 1.49 1.48
1.44 1.50 1.46 1.49 1.49 1.05 1.03 1.03 1.00 1.05 2.40 2.46 2.43 2.45 2.43 1.53 1.53 1.53 1.53 1.53 2.92 2.97 2.95 2.98 2.94
100.0 100.0 98.0 100.0 100.7 101.4 101.4 100.1 100.1 99.3 100.5 99.7 99.5 99.3 96.5 100.3 100.0 99.7 100.7 99.3 94.1 91.4 91.4 92.2 94.4 101.1 101.7 100.5 101.1 102.4 98.2 98.3 98.2 98.2 98.3
1.5
99.7
1.0
0.0978 0.0970 0.0991 0.0981 0.0973
0.1
99.6
2.0
Glucose
0.938
1.46 1.52 1.51 1.50 1.50
1.5
99.9
0.5
0.0975 0.0967 0.0988 0.0978 0.0970
0.1
98.2
0.1
Sucrose
1.46
1.45 1.51 1.50 1.50 1.50
1.5
100.0
0.5
0.0981 0.0973 0.0994 0.0984 0.0976
0.114 0.110 0.112 0.112 0.114 1.50
0.1
92.7
1.6
Fructose
0.0231
1.46 1.52 1.51 1.51 1.51
1.57 1.54 1.55 1.57
1.5
101.4
0.7
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