SPSFAM ERP
Table AI-2-21 . Mince All Analytes Spike Results Analyte SAMPLE ID Approx. Spiking level (%) Actual Spiking level (%) Average Innate level (%)
Total Recovery (%)
Mean Recovery n=3 (%)
%RSD r n=3
Measured Result (%)
7026662 7026663 7026664 7026665 7026666 7026667 7026662 7026663 7026664 7026665 7026666 7026667 7026662 7026663 7026664 7026665 7026666 7026667 7026662 7026663 7026664 7026665 7026666 7026667 7026662 7026663 7026664 7026665 7026666 7026667 7026662 7026663 7026664 7026665 7026666 7026667 7026662 7026663 7026664 7026665 7026666 7026667
0.0965 0.0976 0.0975
0.0914 0.0894 0.0936
94.7 91.6 96.0 97.9 98.6
0.1
94.1
2.4
Galactose
0
1.46 1.48 1.48
1.43 1.46 1.48
1.5
98.8
1.1
100.0 97.0 102.2 100.5 95.4 97.3 96.7 98.9 106.7 93.2 94.0 96.0 96.0 94.2 103.3 96.3 92.5 94.5 96.5 105.5 102.6 100.4
0.0969 0.0980 0.0979
0.224 0.237 0.233
0.1
99.9
2.7
Glucose
0.134
1.47 1.48 1.49
1.53 1.57 1.57
1.5
96.5
1.0
0.0975 0.0986 0.0985
0.137 0.149 0.130
0.1
99.6
6.8
Sucrose
0.0410
1.48 1.49 1.50
1.43 1.47 1.48
1.5
95.3
1.2
0.0968 0.0979 0.0978
0.132 0.146 0.136 1.39
0.1
97.9
4.9
Fructose
0.0434
1.46 1.48 1.49
1.5
1.44 1.48
94.5
2.1
0.0957 0.0968 0.0967
0.101 0.0993 0.0971
0.1
102.8
2.5
Lactose
0
1.45 1.47 1.47
1.42 1.46 1.48
97.9 99.3
1.5
99.3
1.4
100.7 101.3
0.0927 0.0938 0.0937
0.0939 0.0923 0.0854
98.4 91.1
0.1
96.9
5.4
Isomaltulose
0
1.40 1.42 1.43
1.44 1.47 1.48
102.9 103.5 103.5 98.3 100.7 94.1 101.0 101.7 100.9
1.5
103.3
0.3
0.0915 0.0925 0.0924
0.0966 0.100 0.0933
0.1
97.7
3.4
Maltose
0.00676
1.38 1.40 1.41
1.40 1.43 1.43
1.5
101.2
0.4
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