SPSFAM ERP

Table AI-2-41 . Premix Lactose Spike Results Sample ID Approx. Spiking level (%) Spike Level Added (%) Average Innate level (%)

Total Recovery (%)

Mean Recovery n=3 (%)

Measured Result (%)

%RSD r n=3

89.9 87.3 88.1 89.4 89.0 87.9

5907396-1 5907396-2 5907396-3 5907396-4 5907396-5 5907396-6

1.59 1.58 1.59 2.35 2.37 2.39

1.43 1.38 1.40 2.10 2.11 2.10

88.4

1.5

1.5

0.00

88.8

2.25

0.9

Bold indicates individual result outside SMPR criterion Table AI-2-42 . Premix Isomaltulose Spike Results Sample ID Approx. Spiking level (%) Spike Level Added (%) Average Innate level (%) Measured Result (%)

Total Recovery (%)

Mean Recovery n=3 (%)

%RSD r n=3

5907396-1 5907396-2 5907396-3 5907396-4 5907396-5 5907396-6

1.52 1.52 1.53 2.26 2.27 2.30

1.47 1.43 1.44 2.11 2.12 2.13

96.7 94.1 94.1 93.4 93.4 92.6

1.5

95.0

1.6

0.00

2.25

93.1

0.5

Table AI-2-43 . Premix Maltose Spike Results Sample ID Approx. Spiking level (%) Spike Level Added (%) Average Innate level (%)

Total Recovery (%)

Mean Recovery n=3 (%)

Measured Result (%)

%RSD r n=3

5907396-1 5907396-2 5907396-3 5907396-4 5907396-5 5907396-6

1.50 1.50 1.51 2.23 2.25 2.27

1.56 1.54 1.55 2.25 2.28 2.26

95.6 94.4 94.4 95.3 95.7 94.1

1.6

94.8

0.7

0.132

2.3

95.0

0.9