SPSFAM ERP

Table AI-2-45 . Dry Dog Food Galactose Spike Results Sample ID Approx. Spiking level (%) Spike Level Added (%) Average Innate level (%) Measured Result (%)

Total Recovery (%)

Mean Recovery n=3 (%)

%RSD r n=3

5907390-1 5907390-2 5907390-3 5907390-4 5907390-5 5907390-6 5907390-7 5907390-8 5907390-9

0.0987 0.0979 0.0990

0.102 0.097 0.101 1.99 1.98 1.98 2.96 2.95 2.94

103.3 99.1 102.0 100.5 100.5 100.0 99.3 100.0 99.0

0.1

101.5

2.1

1.98 1.97 1.98 2.98 2.95 2.97

0.00

2

100.3

0.3

3

99.4

0.5

Table AI-2-46 . Dry Dog Food Glucose Spike Results Sample ID Approx. Spiking level (%) Spike Level Added (%) Average Innate level (%)

Total Recovery (%)

Mean Recovery n=3 (%)

Measured Result (%)

%RSD r n=3

5907390-4 5907390-5 5907390-6 5907390-7 5907390-8 5907390-9

1.97 1.96 1.97 2.96 2.93 2.96

2.96 3.07 2.97 3.95 3.94 3.96

94.9 98.7 95.2 96.1 96.6 96.4

3

96.3

2.2

1.15

4

96.4

0.3

Table AI-2-47 . Dry Dog Food Sucrose Spike Results Sample ID Approx. Spiking level (%) Spike Level Added (%) Average Innate level (%)

Total Recovery (%)

Mean Recovery n=3 (%)

Measured Result (%)

%RSD r n=3

5907390-4 5907390-5 5907390-6 5907390-7 5907390-8 5907390-9

2.00 1.99 2.00 3.00 2.98 3.00

3.88 3.97 3.88 4.95 4.83 4.85

98.0 100.5 98.0 99.8 97.8 97.8

4

98.8

1.5

1.96

5

98.5

1.2

Table AI-2-48 . Dry Dog Food Fructose Spike Results Sample ID Approx. Spiking level (%) Spike Level Added (%) Average Innate level (%)

Total Recovery (%)

Mean Recovery n=3 (%)

Measured Result (%)

%RSD r n=3

5907390-4 5907390-5 5907390-6 5907390-7 5907390-8 5907390-9

2.01 2.01 2.01 3.02 3.00 3.02

3.46 3.67 3.45 4.64 4.62 4.56

99.4 105.5 99.1 103.3 103.4 101.6

3.5

101.3

3.6

1.47

4.5

102.8

1.0

Table AI-2-49 . Dry Dog Food Lactose Spike Results Sample ID Approx. Spiking level (%) Spike Level Added (%) Average Innate level (%)

Total Recovery (%)

Mean Recovery n=3 (%)

Measured Result (%)

%RSD r n=3

5907390-1 5907390-2 5907390-3 5907390-4 5907390-5 5907390-6 5907390-7 5907390-8 5907390-9

0.0994 0.0986 0.100

0.102 0.101 0.101 1.97 1.94 1.98 2.90 2.93 2.91

102.6 102.4 101.0 99.0 97.5 99.0 96.7 98.7 97.0

0.1

102.0

0.9

1.99 1.99 2.00 3.00 2.97 3.00

2

98.5

0.9

0.00

3

97.5

1.1