SPSFAM ERP

Table AI-2-50 . Dry Dog Food Isomaltulose Spike Results Sample ID Approx. Spiking level (%) Spike Level Added (%) Average Innate level (%) Measured Result (%)

Total Recovery (%)

Mean Recovery n=3 (%)

%RSD r n=3

140.5 144.8 147.3 106.8 106.8 107.3 103.1 103.9 103.1

5907390-1 5907390-2 5907390-3 5907390-4 5907390-5 5907390-6 5907390-7 5907390-8 5907390-9

0.0954 0.0946 0.0957

0.134 0.137 0.141 2.04 2.04 2.06 2.97 2.96 2.96

144.2

0.1

2.4

1.91 1.91 1.92 2.88 2.85 2.87

0.00

2

107.0

0.3

3

103.4

0.4

Bold indicates individual result outside SMPR criterion Table AI-2-51 . Dry Dog Food Maltose Spike Results

Approx. Spiking level (%)

Average Innate level (%)

Total Recovery (%)

Mean Recovery n=3 (%)

Spike Level Added (%)

Measured Result (%)

%RSD r n=3

Sample ID

5907390-1 5907390-2 5907390-3 5907390-4 5907390-5 5907390-6 5907390-7 5907390-8 5907390-9

0.0942 0.0934 0.0945

0.186 0.188 0.187

104.7 106.3 105.1 100.3 100.8 100.6 101.6 100.6 99.3

0.19

105.4

0.8

1.89 1.88 1.89 2.84 2.81 2.84

1.96 1.97 1.99 2.94 2.94 2.94

2

100.1

0.8

0.0834

3

100.9

0.6