SPSFAM ERP

Table AI-2-60 . Horse Feed Isomaltulose Spike Results Sample ID Approx. Spiking level (%) Spike Level Added (%) Average Innate level (%) Measured Result (%)

Total Recovery (%)

Mean Recovery n=3 (%)

%RSD r n=3

5907391-4 5907391-5 5907391-6 5907391-7 5907391-8 5907391-9

2.47 2.47 2.49 3.83 3.82 3.81

2.71 2.78 2.76 4.19 4.23 4.23

109.7 112.6 110.8 109.4 110.7 111.0

111.0

2.5

1.3

0.00

110.4

4

0.8

Bold indicates individual result outside SMPR criterion Table AI-2-61 . Horse Feed Maltose Spike Results Sample ID Approx. Spiking level (%) Spike Level Added (%) Average Innate level (%) Measured Result (%)

Total Recovery (%)

Mean Recovery n=3 (%)

%RSD r n=3

5907391-4 5907391-5 5907391-6 5907391-7 5907391-8 5907391-9

2.44 2.44 2.45 3.78 3.77 3.76

2.58 2.58 2.57 4.00 4.01 4.01

100.6 100.6 99.8 102.5 103.0 103.2

2.5

100.3

0.5

0.124

4

102.9

0.4

Table AI-2-62 . Swine Feed Galactose Spike Results Sample ID Approx. Spiking level (%) Spike Level Added (%) Average Innate level (%)

Total Recovery (%)

Mean Recovery n=3 (%)

Measured Result (%)

%RSD r n=3

5907392-1 5907392-2 5907392-3 5907392-4 5907392-5 5907392-6 5907392-7 5907392-8 5907392-9

0.0988 0.0991 0.0976

0.124 0.120 0.119

106.4 102.7 103.2 100.1

0.1

104.1

1.9

1.98 1.98 1.98 2.97 2.97 2.95

2.00 1.99 1.99 2.99 3.00 2.96

0.0177

99.6 99.6

2

99.8

0.3

100.1 100.4

3

100.1

0.3

99.7

Table AI-2-63 . Swine Feed Glucose Spike Results Sample ID Approx. Spiking level (%) Spike Level Added (%) Average Innate level (%)

Total Recovery (%)

Mean Recovery n=3 (%)

Measured Result (%)

%RSD r n=3

5907392-4 5907392-5 5907392-6 5907392-7 5907392-8 5907392-9

1.97 1.96 1.97 2.95 2.95 2.94

2.30 2.34 2.38 3.34 3.39 3.37

99.9

102.0 103.3 101.7 103.3 103.0

101.7

1.7

2.3

0.333

3.3

102.7

0.8