SPSFAM ERP

Table 14. Precision obtained at the LOQ spiking level of 0.1% for the 7 analytes

Repeatability (n=3), Intermediate Precision (n=5 or 8), or Reproducibility (n=6)

Matrix

Replicates

Galactose

Glucose

Sucrose

Fructose

Lactose

Isomaltulose

Maltose

Peanut Butter

6 3 3 3 3 3 3 3 3 3 8 5 5 5 3 3

5.3 1.2 1.4 1.2 2.1 0.6 1.9 3.0 1.8 3.0 4.8 3.6 2.1 2.4 0.1 2.4 2.6 -

1.6 7.4 3.5 1.1

-

3.2 2.0 1.5 0.2

2.6 2.8 1.9 1.6 0.9 2.4 3.2 1.4 6.6 2.8 0.9 2.1 2.5 0.2 3.3 2.7 - -

7.4 3.7 3.2 3.9 2.4 1.3 1.9 4.7 1.3 4.1 6.2 4.5 3.0 3.3 5.4 1.4 8.7 4.6

6.4 1.4 1.0 1.7 0.6 0.5 2.9 1.8 3.7 1.3 1.8 2.4 3.4 1.0 - -

Baking chocolate Spinach Palm Oil

2.1

-

1.6

Dry dog food Horse feed Swine feed Milk replacer Dry cat food Wet cat food

- - - -

- - -

- - -

3.7

0.7 0.5 2.5 6.5 3.9 2.5 1.6 4.9 0.7 7.7 3.2

0.3 0.9 2.8 7.9 4.4 2.0 2.7 1.5 3.9 3.2

-

1.9 4.8 0.8 0.4 0.1 6.8 1.0

Tuna

Salami Turkey Mince Protein Powder Tablet Ham

6

-

1.4 1

Weighted Average

2.3

2.4

– = Not Applicable 1 Only one lab with three replicates for Maltose LOQ spikes in Tablet matrix Bold indicates individual result outside AOAC 2018.001 SMPR [1] .