SPSFAM ERP

Table AI-2-1 . Lemon Juice Galactose Spike Results

Spike Level Added (%)

Average Innate level (%)

Total Recovery (%)

Mean Recovery n=3 (%)

Sample ID

Approx.Spiking level (%)

Measured Result (%)

%RSD r n=3

Mean Recovery

%RSD R n=11,12

Site

BC BC BC

6196413 6196414 6196415 6345733 6345734 6345735

HAR HAR HAR

0.491 0.494 0.491

0.488 0.484 0.481

99.4 98.0 98.0

0.000

98.5

0.8

MSN 5907383- 1 MSN 5907383- 2 MSN 5907383- 3

0.499

0.477

95.6

97.5

1.4

0.5

0.499

0.478

95.8

0.000

95.9

0.4

0.491

0.473

96.3

5907383- 1 5907383- 2 5907383- 3 6196416 6196417 6196418 6345736 6345737 6345738

SGP

0.491

0.485

98.8

SGP

0.487

0.479

98.4

0.000

98.1

1.0

SGP

0.499

0.484

97.0

BC BC BC

HAR HAR HAR

0.782 0.791 0.788

0.763 0.739 0.769

97.6 93.4 97.6

0.000

96.2

2.5

MSN 5907383- 4 MSN 5907383- 5 MSN 5907383- 6

0.797

0.762

95.6

0.75

97.0

2.3

0.798

0.755

94.6

0.000

95.1

0.7

1.42

177.8

0.800

5907383- 4 5907383- 5 5907383- 6

0.794

0.790

99.5

SGP

0.000

99.1

0.5

SGP

0.786

0.780

99.2

SGP 98.5 Galactose was not tested for accuracy at the Battle Creek site due to lack of standard material. Bold type indicates outlier omitted from data summary. 0.796 0.784