KRA-01
FDA/ORA/ORS
LIB #4578 20 of 25
Figure 16: a) Negative Control - Total Ion Chromatogram (TIC)
b) Negative Control Reconstructed Ion Chromatogram (RIC)
Kraton_27Dec12_A12 - TIC - SM: 5 RT: 5.00 - 14.99
NL: 3.65E2
RT: 11.55
10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 Relative Intensity
a
12.24
7.86
10.82
5.46
6.95
10.03
7.45
13.18
5.78
6.65
9.56
14.37
11.12
12.70
8.95
6.29
8.52
10.31
0 5
6
7
8
9
10
11
12
13
14
Time (min)
RT: 10.50 - 15.00
RT: 10.50 - 15.00
NL: 6.17E2 TIC F: + c ESI SRM ms2 399.200
11.55
NL: 3.74E2 m/z= 173.90-174.10 F: + c ESI
11.55
100
10 20 30 40 50 60 70 80 90 100
SRM ms2 399.200 [159.099-159.101, 174.099-174.101,
b
[159.099-159.101, 174.099-174.101,
95
238.199-238.201] MS Kraton_27Dec12_A12
238.199-238.201] MS Kraton_27Dec12_A12
SRM 399.2->174.1 Negative Contol Mitragynine Rt=11.53
90
Total Ion Chromatogram (TIC) Negative Contol Mitragynine Rt=11.53
85
11.12
12.32
11.71
12.70
80
10.82
11.83
14.61
75
14.56 13.50 13.99
70
10 20 30 40 50 60 70 80 90 100 Relative Abundance 0 10.82
NL: 6.17E2 TIC F: + c ESI SRM ms2 399.200 [159.099-159.101, 174.099-174.101,
12.24
11.55
65
60
238.199-238.201] MS Kraton_27Dec12_A12
11.63
55
SRM 399.2->159.1 Negative Contol Mitragynine Rt=11.53
11.63
50
13.18
11.48
12.32
45
14.89
10.82
13.89
12.04
Relative Abundance
13.98
11.51
13.73
40
13.18
11.48
35
0 10 20 30 40 50 60 70 80 90 100 0
12.32
NL: 2.52E2 m/z= 238.00-238.20 F: + c ESI
11.63
14.89
12.70
30
11.12
SRM ms2 399.200 [159.099-159.101, 174.099-174.101,
13.89
12.04
13.98
25
14.89
238.199-238.201] MS Kraton_27Dec12_A12
14.37
SRM 399.2->238.1 Negative Contol Mitragynine Rt=11.53
20
13.98
12.04
13.73
15
11.48
13.89 14.37
10
11.25
13.63
12.95
12.27
5
13.09
0
11
12
13
14
15
14
15
11
12
13
Time (min)
Time (min)
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