SPDS SET 2: ASH-01

NATURAL REMEDIES PVT LIMITED QUALITY CONTROL DEPARTMENT

Acquired by Sample Name

: Admin

: Withania somnifera ext

Sample ID

: WS - RD / 1045

Vail #

: 17

Injection Volume Data File Name Method File Name Batch File Name Report File Name Data Acquired Data Processed

: 20 uL

: Quan004.lcd

: Withaina.met.lcm : Batch 01.lcb : Calibration.lcr

: 1/15/2007 10:18:22 AM : 1/23/2007 2:49:54 AM

D:\LC2010AHT\2007\Method validation\Withania somnifera\Jan 2007\Quan004.lcd

mV

500

1Det.A Ch1

400

300

3

200

4

1

5

100

2

6

0

0

5

10

15

20

25

30

35

40

45

min

Det.A Ch1/227nm 1

Detector A Ch1 227nm Peak # Ret. Time

Area

Height

Area %

Name

1 2 3 4 5 6 Total

15.516 19.698 20.371 21.392 22.248 25.536

699116 521948 1573294 1123326 539632 183000 4640315

126309 74525 218195 169172 98989 31526 718716

15.066 11.248 33.905 24.208 11.629 3.944 100.000

Withanoside IV Withanoside V Withaferin A 12- Deoxy withastramonolide

Withanollide A Withanolide B

D:\LC2010AHT\2007\Method validation\Withania somnifera\Jan 2007\Quan004.lcd