SPDS SET 2: ASH-01

NATURAL REMEDIES PVT LIMITED QUALITY CONTROL DEPARTMENT

Acquired by Sample Name

: Admin

: Withania somnifera ext

Sample ID

: WS - RD / 1045

Vail #

: 28

Injection Volume Data File Name Method File Name Batch File Name Report File Name Data Acquired Data Processed

: 20 uL

: SSR003.lcd

: Withaina.met.lcm : Batch 01.lcb : Calibration.lcr

: 1/15/2007 6:41:31 PM : 1/23/2007 3:29:31 AM

D:\LC2010AHT\2007\Method validation\Withania somnifera\Jan 2007\SSR003.lcd

1Det.A Ch1

500

3

4

400

5

300

6

200

1

100

2

0

0

5

10

15

20

25

30

35

40

45

min

Det.A Ch1/227nm

Detector A Ch1 227nm Peak # Ret. Time

Area

Height

Area %

Name

1 2 3 4 5 6 Total

15.423 19.583 20.267 21.295 22.161 25.475

918311 454914

157419 64877 500231 500734 357485 259646 1840392

8.002 3.964

Withanoside IV Withanoside V Withaferin A 12- Deoxy withastramonolide

3469556 3040941 2085779 1506717 11476218

30.233 26.498 18.175 13.129 100.000

Withanollide A Withanolide B

D:\LC2010AHT\2007\Method validation\Withania somnifera\Jan 2007\SSR003.lcd