SPDS SET 2: ASH-01

QUALITY CONTROL DEPARTMENT

Name of Sample Method Name Data File Name

: Withania somnifera : RD - 1170 : C:\Methods\WITHANIA.met

: D:\LC10-ATvp\2007\Method validation\Apr 2007\020407\S6-Rep1

Vial No

: 10007

Injection Volume

: 20

Date & Time

: 4/4/07 4:22:45 PM

0.4

0.3

23.042

17.217

23.908

0.2

Volts

21.400

0.1

27.033

0.0

22.067

0

5

10

15

20

25

30

35

40

45

Minutes

Detector A - 1 (227nm)

Pk # Retention Time Name

Area Area Percent

1 2 3 4 5 6

17.217 21.400 22.067 23.042 23.908 27.033

WIthanoside IV Withanoside V

1093704 749692 2479748 972595 1268626 291589

15.95 10.93 36.17 14.19 18.50

Withaferin A

Withastramonolide

Withanolide A Withanolide B

4.25

Totals

6855954

100.00