SPIFAN Nutrients ERP Book_9-29-15

GOS-02 SLV FOR ERP USE ONLY DO NOT DISTRIBUTE

Single Lab Validation Report for GOS in Infant Formula and Adult Nutritionals

Spike-Recovery: Sample 11 Child Formula Powder

GOS Spike Level Measured GOS Recovery Average RSD (g/100g) (g/100g) (%) (%) (%)

Date* Instrument** GOS

11-02-2015 ICS 3000 11-02-2015 ICS 3000 18-02-2015 ICS 5000 18-02-2015 ICS 5000 09-06-2015 ICS 3000 09-06-2015 ICS 3000 11-02-2015 ICS 3000 11-02-2015 ICS 3000 18-02-2015 ICS 5000 18-02-2015 ICS 5000 10-06-2015 ICS 3000 10-06-2015 ICS 3000 11-02-2015 ICS 3000 11-02-2015 ICS 3000 18-02-2015 ICS 5000 18-02-2015 ICS 5000 10-06-2015 ICS 3000 10-06-2015 ICS 3000 11-02-2015 ICS 3000 11-02-2015 ICS 3000 18-02-2015 ICS 5000 18-02-2015 ICS 5000 10-06-2015 ICS 3000 10-06-2015 ICS 3000

0.021 0.021 0.021 0.021 0.021 0.021 0.133 0.133 0.139 0.139 0.135 0.135 0.371 0.371 0.378 0.378 0.375 0.375 0.593 0.593 0.616 0.616 0.599 0.599

0.019 0.017 0.014 0.018 0.022 0.025 0.117 0.115 0.119 0.117 0.109 0.112 0.337 0.340 0.324 0.342 0.284 0.289 0.507 0.520 0.497 0.521 0.497 0.508

90 79 69 87

Vivinal

90

18.5

100 117

88 87 86 84 81 83 91 92 86 90 76 77 85 88 81 85 83 85

Clasado

85

3.3

Vivinal

85

8.5

Clasado

84

2.8

* Date = date of preparative separation ** Instrument = instrument used for quantification

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