SPIFAN Nutrients ERP Book_9-29-15

Carn-06 (Validation Report-Addendum) FOR ERP USE ONLY DO NOT DISTRIBUTE

Day 1 Day 2 Day 3

2 311,5675077 155,7837538

4,2559746

2 311,300509 155,6502545 0,104950096 2 314,2306529 157,1153265 0,087835148

ANAVA Source of Variation

SS

df

MS

F

P-value

F crit

Between Groups Within Groups

2,624895781 4,448759844 7,073655625 -0,085236029 1,397683919

2 1,312447891 0,88504298 0,498761 9,552094

3 1,482919948

Total Sl^2 SR^2

5

Reproducibility (SR) Repeatability (Sr)

1,18 mg/kg 1,22 mg/kg

RSD%

0,8 % 0,8 %

Sample name Adult Nut. RFT High Fat Sample nr. 487-2014-04020202

Rep 1 (mg/kg) Rep 2 (mg/kg) 220,6765481 218,1061917 220,4129711 223,8276604 221,6249524 225,4660592

Average of all days

Day 1 Day 2 Day 3

221,69 mg/kg

Anava: Single faktor Summary Groups

Count

Sum

Average

Variance

Day 1 Day 2 Day 3

2 438,7827398 219,3913699 3,303365957 2 444,2406315 222,1203157 5,830051435 2 447,0910115 223,5455058 7,377050819

ANAVA Source of Variation

SS

df

MS

F

P-value

F crit

Between Groups Within Groups

17,82343769 16,51046821 34,3339059 1,704114721 7,207604125

2 8,911718846 1,619285183 0,333468 9,552094

3 5,503489404

Total Sl^2 SR^2

5

Reproducibility (SR) Repeatability (Sr)

2,68 mg/kg 2,35 mg/kg

RSD%

1,2 % 1,1 %

Free Carnitne:

Sample name

Lot#

Day 1 (mg/kg)

Day 2 (mg/kg)

Day 3 (mg/kg)

Child Formula Powder Child Formula Powder Infant Element Powder Infant Element Powder Adult Nut. RFT High Pro- tein Adult Nut. RFT High Pro- tein Adult Nut. RFT High Fat Adult Nut. RFT High Fat Infant Formula RFT, Milk Based

00411RF00 00411RF00 00402RF00 00402RF00 00415RF00 00415RF00 00407RF00 00407RF00 Spifan Blank Milk Form

Rep. 1 Rep. 2 Rep. 1 Rep. 2 Rep. 1 Rep. 2 Rep. 1 Rep. 2 Rep. 1

1,254160016 1,517589024 1,708356171 1,597505237 0,281750232 0,630450654 0,51285317 0,270410237 0,353030884 0,402888636 0,405091552 0,382089031 0,456936563 0,569845912 0,579822064 0,540715732 25,67551927 25,29927744

1,431514476 1,680537147 0,409483725 0,224943737 0,323884232 0,337483995 0,339190282 0,476087797 24,48829302