SPIFAN Nutrients ERP Book_9-29-15

Carn-06 (Validation Report-Addendum) FOR ERP USE ONLY DO NOT DISTRIBUTE

Source of Variation

SS

df

MS

F

P-value

F crit

Between Groups Within Groups

4,500056545 12,64116307 17,14121962 -0,981846376 3,231874648

2 2,250028272 0,533977 0,633312372 9,552094496

3 4,213721024

Total Sl^2 SR^2

5

Reproducibility (SR) Repeatability (Sr)

1,797741541 mg/kg 2,052735011 mg/kg

RSD%

1,3 % 1,5 %

Sample name: Infant Formula, Milk Based

Eurofins Sample nr.: 487-2014-04020198

Rep. 1 (mg/kg) Rep. 2 (mg/kg) 141,8624491 139,4849933 137,6616407 138,1792715 134,8425119 138,7746267

Average of all days 138,47 mg/kg

Day 1 Day 2 Day 3

Anava: Single faktor Summary Groups

Count

Sum

Average

Variance

Day 1 Day 2 Day 3

2 281,3474424 140,6737212 2,826148 2 275,8409122 137,9204561 0,133971 2 273,6171386 136,8085693 7,730763

ANAVA Source of Variation

SS

df

MS

F

P-value

F crit

Between Groups Within Groups

15,83744005 10,69088193 26,52832199 2,177546358 5,741173669

2 7,918720026 2,222095

0,25583245 9,552094496

3 3,563627311

Total Sl^2 SR^2

5

Reproducibility (SR) Repeatability (Sr)

2,396074638 mg/kg 1,887757217 mg/kg

RSD%

1,7 % 1,4 %

Sample name: Infant Formula, Soy Based

Eurofins Sample nr.: 487-2014-04020199

Rep. 1 (mg/kg) Rep. 2 (mg/kg) 81,7539561 83,11756666 80,33855374 80,31946507 80,85855958 83,13839601

Average of all days 81,59 mg/kg

Day 1 Day 2 Day 3

Anava: Single faktor Summary Groups

Count

Sum

Average

Variance

Day 1 Day 2 Day 3

2 164,8715228 82,43576138 0,929717

2 160,6580188 2 163,9969556

80,3290094 0,000182 81,9984778 2,598827

ANAVA Source of Variation

SS

df

MS

F

P-value

F crit

Between Groups Within Groups

4,944497028 3,52872613

2 2,472248514 3 1,176242043

2,10182 0,268753398 9,552094496

Total

8,473223158

5