SPIFAN Nutrients ERP Book_9-29-15

GOS-02 SLV FOR ERP USE ONLY DO NOT DISTRIBUTE

Single Lab Validation Report for GOS in Infant Formula and Adult Nutritionals

Spike-Recovery: Sample 7 Adult Nutritional Powder Milk Protein Based

GOS Spike Level Measured GOS Recovery Average RSD (g/100g) (g/100g) (%) (%) (%)

Date* Instrument** GOS

10-02-2015 ICS 3000

0.021

0.01558

74

10-02-2015 ICS 3000

0.021

0.02218

105

17-02-2015 ICS 5000 17-02-2015 ICS 5000 08-06-2015 ICS 3000 08-06-2015 ICS 3000 10-02-2015 ICS 3000 10-02-2015 ICS 3000 17-02-2015 ICS 5000 17-02-2015 ICS 5000 09-06-2015 ICS 3000 09-06-2015 ICS 3000 10-02-2015 ICS 3000 10-02-2015 ICS 3000 17-02-2015 ICS 5000 17-02-2015 ICS 5000 08-06-2015 ICS 3000 08-06-2015 ICS 3000 10-02-2015 ICS 3000 10-02-2015 ICS 3000 17-02-2015 ICS 5000 17-02-2015 ICS 5000 09-06-2015 ICS 3000 09-06-2015 ICS 3000

0.021 0.021 0.021 0.021 0.132 0.132 0.137 0.137 0.136 0.136 0.379 0.379 0.374 0.374 0.376 0.376 0.594 0.594 0.615 0.615 0.596 0.596

0.02023 0.01908 0.01875 0.01843 0.11689 0.10045 0.12498 0.12783 0.10475 0.10662

97 91 89 87 89 76 91 93 77 79 88 90 81 87 87 87 89 91 84 85 80 82

Vivinal

91

11.5

Clasado

84

9.0

0.333 0.340 0.303 0.325 0.327 0.327 0.532 0.541 0.518 0.523 0.478 0.488

Vivinal

86

3.4

Clasado

85

5.0

* Date = date of preparative separation ** Instrument = instrument used for quantification

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