SPIFAN Nutrients ERP Book_9-29-15

GOS-02 SLV FOR ERP USE ONLY DO NOT DISTRIBUTE

Single Lab Validation Report for GOS in Infant Formula and Adult Nutritionals

Spike-Recovery: Sample 10 Adult Nutritional Powder Low Fat

GOS Spike Level Measured GOS Recovery Average RSD (g/100g) (g/100g) (%) (%) (%)

Date* Instrument** GOS

10-02-2015 ICS 3000 10-02-2015 ICS 3000 18-02-2015 ICS 5000 18-02-2015 ICS 5000 09-06-2015 ICS 3000 09-06-2015 ICS 3000 10-02-2015 ICS 3000 10-02-2015 ICS 3000 18-02-2015 ICS 5000 18-02-2015 ICS 5000 09-06-2015 ICS 3000 09-06-2015 ICS 3000 10-02-2015 ICS 3000 10-02-2015 ICS 3000 18-02-2015 ICS 5000 18-02-2015 ICS 5000 09-06-2015 ICS 3000 09-06-2015 ICS 3000 10-02-2015 ICS 3000 10-02-2015 ICS 3000 18-02-2015 ICS 5000 18-02-2015 ICS 5000 09-06-2015 ICS 3000 09-06-2015 ICS 3000

0.023 0.023 0.023 0.023 0.023 0.023 0.125 0.125 0.126 0.126 0.126 0.126 0.402 0.402 0.416 0.416 0.399 0.399 0.555 0.555 0.559 0.559 0.566 0.566

0.019 0.026 0.022 0.023 0.023 0.022 0.116 0.116 0.109 0.118 0.103 0.115 0.345 0.347 0.380 0.337 0.345 0.362 0.495 0.490 0.541 0.507 0.461 0.463

82

113

94

Clasado

98

10.3

101

99 99

93 92 86 94 82 91 86 86 91 81 86 91 89 88 97 91 81 82

Vivinal

90

5.2

Clasado

87

4.3

Vivinal

88

6.6

* Date = date of preparative separation ** Instrument = instrument used for quantification

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