SPSFAM ERP

Table AI-2-7 . Lemon Juice Maltose Spike Results

Spike Level Added (%) 0.502 0.502 0.501 0.467 0.470 0.467 0.465 0.461 0.473 0.784 0.790 0.788 0.744 0.752 0.749

Approx. Spiking level (%)

Average Innate level (%)

Total Recovery (%)

Mean Recovery n=3 (%)

Measured Result (%)

%RSD r n=3

Mean Recovery

%RSD R n=12

Site

Sample ID

BC BC BC

6196413 6196414 6196415 6345733 6345734 6345735

0.484 0.484 0.491 0.457 0.458 0.457

96.4 96.4 98.0 97.9 97.4 97.9

96.9

1.0

0.000

HAR HAR HAR MSN MSN MSN SGP SGP SGP HAR HAR HAR MSN MSN MSN SGP SGP SGP BC BC BC

0.000

97.7

0.3

98.3

1.9

0.5

5907383-1 5907383-2 5907383-3 5907383-1 5907383-2 5907383-3

0.456 0.472 0.473 0.761 0.773 0.771 0.725 0.718 0.737

98.1

100.2

2.2

0.000

102.4 100.0 97.1 97.8 97.8 97.4 95.5 98.3

6196416 6196417 6196418 6345736 6345737 6345738

0.000

97.6

0.4

0.000

97.1

1.5

0.75

98.4

1.8

5907383-4 5907383-5 5907383-6 5907383-4 5907383-5 5907383-6

0.752 0.744 0.754

0.751 0.753 0.755

99.9

0.000

100.4

0.7

101.2

100.1 Maltose was not tested for accuracy at the Madison site due to lack of standard material.