SPSFAM ERP
Table AI-2-12 . Spinach All Analytes Spike Results Analyte Sample ID
Approx. Spiking level (%)
Actual Spiking level (%) 0.0977 0.0993 0.0994
Average Innate level (%)
Measured Result (%)
Total Recovery (%)
Avg. Recovery n=3 (%)
%RSD r n=3
7078241 7078243 7078244 7078245 7078246 7078247 7078241 7078243 7078244 7078245 7078246 7078247 7078241 7078243 7078244 7078245 7078246 7078247 7078241 7078243 7078244 7078245 7078246 7078247 7078241 7078243 7078244 7078245 7078246 7078247 7078241 7078243 7078244 7078245 7078246 7078247 7078241 7078243 7078244 7078245 7078246 7078247
0.104 0.105 0.103
106.4 105.7 103.6 103.3 102.8 103.4 111.2 103.8 106.4 102.9 102.4 103.0 109.2 99.5 104.2 101.6 100.5 102.2 102.4 99.3 101.8 101.0 101.7 101.7 103.1 99.9 103.2 103.3 100.7 104.1 106.1 100.2 100.5 104.2 100.0 103.5 105.8 105.2 103.7 103.5 101.5 103.6
0.1
105.2
1.4
Galactose
0
1.50 1.45 1.48
1.55 1.49 1.53
1.5
103.2
0.3
0.0972 0.0988 0.0989
0.385 0.361 0.370
0.1
107.1
3.5
Glucose
0.249
1.49 1.44 1.47
1.79 1.73 1.77
1.5
102.8
0.3
0.0989 0.101 0.101
0.415 0.380 0.398 1.83
0.1
104.3
4.7
Sucrose
0.281
1.52 1.47 1.50
1.5
1.76 1.82
101.4
0.9
0.0990 0.101 0.101
0.167 0.164 0.168
0.1
101.2
1.6
Fructose
0.0641
1.52 1.47 1.50
1.60 1.56 1.59
1.5
101.5
0.4
0.0980 0.0997 0.0998
0.101 0.0996 0.103
0.1
102.2
1.8
Lactose
0
1.50 1.46 1.48
1.55 1.47 1.54
1.5
102.7
1.7
0.0934 0.0949 0.0950
0.0991 0.0951 0.0955
0.1
102.3
3.2
Isomaltulose
0
1.43 1.39 1.41
1.49 1.39 1.46
1.5
102.6
2.2
0.0924 0.0939 0.0940
0.0978 0.0988 0.0975
0.1
104.9
1.0
Maltose
0
1.42 1.37 1.40
1.47 1.39 1.45
1.5
102.9
1.2
Bold indicates individual result outside SMPR criterion
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