SPSFAM ERP

Table AI-2-25 . Tuna Maltose Spike Results

Approx.  Spiking level  (%) 

Actual  Spiking level  (%) 

Average  Innate level  (%) 

Measured  Result   (%) 

Total  Recovery  (%) 

Mean  Recovery  n=9 (%) 

%RSD i n=9 

Analyte 

SAMPLE ID 

6834362  6834363  6834364  6839352  6839353  6839355  6847359  6847360  6847361  6834366  6834367  6834368  6839356  6839357  6839359  6847363  6847364  6847366 

0.0928  0.0934  0.0916  0.0928  0.0955  0.0929  0.0934  0.0918  0.0947 

0.0906  0.0932  0.0910  0.0973  0.0966  0.0919  0.147  0.0929  0.103 

97.6  99.8  99.3 

104.8  107.5  104.0 

0.1 

101.2 

3.7 

98.4 

160.1* 

98.1 

Maltose 

0 

1.37  1.42  1.44  1.42  1.37  1.41  1.40  1.37  1.38 

1.38  1.44  1.45  1.48  1.41  1.46  1.44  1.42  1.41 

100.7  101.4  100.7  104.2  102.9  103.5  102.9  103.6  102.2 

1.5 

102.5 

1.3 

* – Dixon outlier excluded, n=8 for 0.1% spike level. Table AI-2-26 . Gummy Galactose Spike Results

Spike Level Added (%)

Approx. Spiking level (%)

Average Innate level (%)

Total Recovery (%)

Mean Recovery n=3 (%)

Measured Result (%)

%RSD r n=3

Sample ID

5907394-1 5907394-2 5907394-3

1.44 1.43 1.44

1.42 1.41 1.43

98.6 98.6 99.3

1.5

0.00

98.8

0.4

Table AI-2-27 . Gummy Glucose Spike Results

Spike Level Added (%)

Approx. Spiking level (%)

Average Innate level (%)

Total Recovery (%)

Mean Recovery n=3 (%)

Measured Result (%)

%RSD r n=3

Sample ID

98.5

5907394-1 5907394-2 5907394-3

1.43 1.42 1.43

6.73 6.84 6.72

100.3

99.1

1.1

6.8

5.40

98.4