SPSFAM ERP

Table AI-2-44 . Protein Powder Drink All Analytes Spike Results

%RSD r n=3

Approx. Spiking level (%)

Actual Spiking level (%)

Average Innate level (%)

Mean Recovery n=3 (%)

Sample ID 7083875 7083876 7083877 7083878 7083879 7083880 7083875 7083876 7083877 7083878 7083879 7083880 7083875 7083876 7083877 7083978 7083979 7083981 7083875 7083876 7083877 7083878 7083879 7083880 7083875 7083876 7083877 7083878 7083879 7083880 7083881 7083882 7083883 7083884 7083885 7083886 7083875 7083876 7083877 7083878 7083879 7083880 7083875 7083876 7083877 7083878 7083879 7083880

Measured Result (%)

Total Recovery (%)

Analyte

0.0975 0.0984 0.0993

0.121 0.122 0.123

100.4 100.5 100.6 102.9 102.1 101.9 100.2 103.0 102.5 104.9 102.2 104.7 106.3 104.3 105.4 104.7 103.4 103.5 102.9 101.7 101.7 100.0 102.3 100.9 102.8 102.1 102.8 103.4 106.2 102.5 105.6 99.2 100.4 98.7 99.9 99.7

0.1

100.5 

0.1 

Galactose

0.0230

1.47 1.48 1.49

1.54 1.53 1.54 2.15 2.21 2.20 3.69 3.60 3.70

1.5

102.2 

0.7 

0.0971 0.0980 0.0989

0.1

101.8 

1.5 

Glucose

2.05

1.47 1.47 1.48

1.5

104.0 

1.4 

0.0988 0.0997 0.100

0.105 0.104 0.106

0.1

105.2 

1.0 

Sucrose

0

1.49 1.50 1.51

1.56 1.55 1.56

103.8 

0.8 

1.5

0.0988 0.0997 0.101

0.165 0.164 0.165

0.1

102.0 

0.7 

Fructose

0.0615

1.49 1.50 1.51

1.54 1.57 1.55 2.65 2.65 2.66 4.13 4.08 4.17 5.22 5.27 5.29 6.77 6.55 6.77

99.3 

0.7 

1.5

0.0979 0.0988 0.0997

0.1

99.8 

0.2 

1.48 1.48 1.50 2.55 2.57 2.55 3.82 3.84 3.85

102.0 

0.9 

1.5

Lactose

2.56

2.6

102.7 

0.5 

3.9

104.7 

2.0 

0.0933 0.0941 0.0950

0.0924 0.0906 0.0926

99.0 96.3 97.5

0.1

97.6 

1.4 

Isomaltulose

0

1.41 1.41 1.43

1.50 1.50 1.53

106.4 106.4 107.0

1.5

106.6 

0.3 

0.0923 0.0931 0.0940

0.253 0.249 0.253

92.6 90.8 92.0 99.9 98.7 99.9

0.1

91.8 

1.0 

Maltose

0.181

1.39 1.40 1.41

1.57 1.56 1.59

1.5

99.5 

0.7